EPA Method 300.0


ALS - Columbia offers EPA Method 300.0 testing at these laboratories:

Jacksonville Jacksonville, Florida Laboratory
Kelso Kelso, Washington Laboratory
Rochester Rochester, New York Laboratory
Simi Valley Simi Valley, California Laboratory
Tucson Tucson, Arizona Laboratory

Method information displayed is provided for informational purposes only. No warranty (express or implied) is made as to the website accuracy, completeness, or applicability (such as the age of a method and whether or not it applies to your project). Please contact us for assistance. Analytical testing dots

PDF IconView Actual EPA Method 300.0 (PDF File)


EPA Method 300.0:
Inorganic Anions by Ion Chromatography. Official Name: Determination of Inorganic Anions by Ion Chromatography

Summary:
A small volume of sample, typically 50-100 uL, is introduced into an ion chromatograph. The anions of interest are separated and measured, using a system comprised of a guard column, separator column, suppressor device, and conductivity detector.

Scope:
Part A of the test method covers the determination of common inorganic anions in drinking water, surface water, mixed domestic and industrial wastewaters, groundwater, reagent waters, solids (after extraction), leachates (when no acetic acid is used). Part B of the test method covers the determination of bromate, chlorate, and chlorite in drinking and reagent waters.

Citation:
Methods for the Determination of Inorganic Substances in Environmental Samples (EPA/600/R-93/100)

Interferences:
(1) Coeluting species (e.g., low-molecular-weight organic acids). (2) High concentration of anions can effect resolution of peaks and elution times. (3) Fluoride is especially sensitive to coeluting species, and "water dip" (corresponding to the elution of water) at low concentrations.

QC Requirements:
Calibration Blank (CB), Quality Control Sample (QCS), Performance Evaluation Sample (PE), Instrument Performance Check Solution (IPC), Laboratory Duplicate (LD), Field Duplicate (FD), Laboratory Fortified Matrix (LFM), Laboratory Fortified Blank (LFB), Laboratory Reagent Blank (LRB), Linear Calibration Range (LCR)

Maximum Holding Time:
Part A: 48 Hours (NO2-N, NO3-N, orthophosphate-P) 28 days (others)Part B: Bromate and Chlorate (28 days) and chlorite (14 days with preservation -- otherwise analyze immediately).

Media:
WATER

Subcategory:
Inorganic

Concentration:
DL - * (* Upper detection limit is defined as the highest calibration point, as determined by analyst.)

Precision:
Precision and accuracy were obtained from a single operator study, analyzing 7 replicate reagent water samples. Additional precision and accuracy data, including data from different matrices, are available in the method.

Detection:
Not explicitly described

Revision Number:
Revision 2.1, August 1993

Test Description:
Chloride - IC

Report Number:
600/4-79-020

Instrument used for this test:
IC

Analytical testing dots
At least 13 analytes can be tested by ALS - Columbia using EPA Method 300.0. Please contact us for all available analytes which can be tested by EPA Method 300.0.

AnalyteCAS Number
Bromide24959-67-9
Chloride16887-00-6
Fluoride16984-48-8
Nitrite as Nitrite14797-65-0
Nitrite as Nitrogen14797-65-0A
Nitrate+Nitrite as NitrogenCASID10034
Nitrate as Nitrate14797-55-8
Nitrate as Nitrogen14797-55-8A
Sulfate14808-79-8
Sulfur7704-34-9
Thiosulfate14383-50-7
Iodide20461-54-5
Orthophosphate as Phosphate14265-44-2





Examples:  8260
TO-15

Examples:  Dioxin
Mercury
Analytical testing dots


<-- Search All Test Methods



Suggestions? The test methods page continues to expand and improve. If you have suggestions for improvement, we would enjoy hearing from you. Please contact the webmaster here.


Analytical testing dots