EPA Method 5050
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EPA Method 5050:
BOMB PREPARATION METHOD FOR SOLID WASTE
The sample is oxidized by combustion in a bomb containing oxygen under pressure. The liberated halogen compounds are absorbed in a sodium carbonate/sodium bicarbonate solution. Approximately 30 to 40 minutes are required to prepare a sample by this method. Samples with a high water content (> 25%) may not combust efficiently and may require the addition of a mineral oil to facilitate combustion. Complete combustion is still not guaranteed for such samples.
This method describes the sample preparation steps necessary to determine total chlorine in solid waste and virgin and used oils, fuels and related materials, including: crankcase, hydraulic, diesel, lubricating and fuel oils, and kerosene by bomb oxidation and titration or ion chromatography. Depending on the analytical finish chosen, other halogens (bromine and fluorine) and other elements (sulfur and nitrogen) may also be determined.
SW-846 Ch 5
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