Columbia Analytical Services

Posts Tagged ‘Analysis’

Low Cost ‘Chinese Drywall’ Testing Available for Elemental Sulfur

Friday, December 11th, 2009

Chinese Drywall Testing for SulfurSimi Valley, Calif. — A low cost testing option is now available from Columbia Analytical for detecting elemental sulfur (S8) in bulk drywall. The testing focuses on orthorhombic cyclooctasulfur (elemental sulfur: S8), a unique marker compound found only in drywall which causes corrosion. The test costs approximately $100 per drywall sample, depending on your project.

Columbia Analytical’s proven method for elemental sulfur uses gas chromatography with electron capture detection (GC/ECD) and allows for rapid turnaround of sample results. The GC/ECD analytical technique offers comparable sensitivity to the GC/MS method also offered by Columbia Analytical, but at a substantially lower cost.

The low cost GC/ECD analysis allows clients to screen a large volume of drywall samples quickly for S8. Because drywall used in home construction can be from mixed sources, submission of multiple samples from one suspect home may be done to reduce the risk of false negative results. In addition, confirmatory analysis of drywall for S8 by GC/MS is still available and may be performed on the same sample as the GC/ECD analysis.

Roughly 5g (approximately 2”x2”) of bulk drywall material is all that is required for this new GC/ECD analysis. Results are reported in units of mg/kg. A result higher than 10 mg/kg is typically indicative of corrosive drywall, making it easy to identify “bad drywall.”

Columbia Analytical’s Research & Development team began laboratory analysis on suspect drywall in spring 2008. They have since analyzed several hundred drywall samples from homeowners, home builders and developers, environmental consultants/industrial hygienists, government agencies and contractors, as well as, domestic and foreign drywall producers as part of their method development.

Columbia Analytical Services, Inc. is an employee-owned, full-service environmental analytical laboratory testing network established in 1986 and headquartered in Kelso, Washington. Their expertise encompasses air, water, dioxin, biological, pharmaceutical, solid and hazardous waste analyses.

For more information on the laboratory analysis of problem drywall, contact Alyson Fortune at 978.501.2735 or visit Columbia Analytical’s website at www.caslab.com.

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Learn more about Chinese drywall testing

Columbia Analytical Develops Protocol for Testing Corrosion and Odor in Chinese Drywall

Thursday, May 21st, 2009

Chinese Drywall Odor TestSIMI VALLEY, California — Columbia Analytical Services, Inc. announces it has established a reliable test protocol for identifying odor and corrosion problems in drywall. The tests identify problems with drywall, generally reported as “Chinese drywall,” that initially affected many homes in the southeastern United States.

“Our team has developed three technically superior and legally-defensible analytical tests related to the drywall problem,” said Michael Tuday, Director of Research and Development at Columbia Analytical’s Simi Valley, California laboratory. “We have been studying the issue and testing both foreign and domestic drywall samples since February, 2008, and are excited to have found a testing solution to isolate this problem.”

The Simi Valley laboratory confirmed that hydrogen sulfide is one of the major contributing agents causing the corrosion. With its characteristic rotten egg smell, hydrogen sulfide is a likely contributor to reported odors in affected homes. Other researchers have also identified iron disulfide (pyrite) and strontium sulfide as possible corrosion culprits, as well.

Researchers at Columbia Analytical also determined the drywall in question contains a naturally occurring allotrope of elemental sulfur and have developed a novel means of quantifying orthorhombic cyclooctasulfur (S8) in drywall via analysis by gas chromatography/mass spectrometry (GC/MS). In tests to-date, this sulfur allotrope is a unique and reliable marker in drywall products causing corrosion problems and has only been found in drywall imported from China.

Columbia Analytical has developed an innovative chamber test procedure for the measurement of hydrogen sulfide at ultra-low levels in suspect drywall. To confirm corrosivity, a jar test is used to document copper corrosion in the presence of test drywall samples.

These laboratory tests may be used to confirm visual home inspections and to demonstrate that corrosion effects are due to drywall and not other items in the home, such as carpets, cleaners, paints, or personal care products.

Columbia Analytical is an employee-owned, full-service environmental analytical network with laboratories and service centers nationwide. The company’s expertise encompasses air, water, dioxin, biological, pharmaceutical, and solid and hazardous waste analyses.

For more information about drywall testing, contact Alyson Fortune at 978.501.2735 or visit Columbia Analytical’s website at www.caslab.com.

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Learn more about Chinese Drywall Testing

Learn more about Low Cost Chinese Drywall Testing…

Learn more about Chinese Drywall Problems

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Anthraquinone Analysis Offered by Columbia Analytical

Wednesday, July 23rd, 2008

The GC-MS is used for testing anthraquinoneColumbia Analytical has completed the implementation of the National Council of Air and Stream Improvement (NCASI) Method AQ-S108.01 for the determination of anthraquinone in pulp and paper products.

In response to California’s listing of anthraquinone with Proposition 65, many companies are proactively having their products tested for anthraquinone in advance of the ruling’s effective date. This procedure is currently being performed by Columbia Analytical as written and released by NCASI.

Columbia Analytical has been in consultation with NCASI scientists over the past year in preparation for this action by the state. This preparation enabled Columbia Analytical to be in position to offer the Gas Chromatography/Mass Spectrometry (GC/MS) procedure in time for pulp and paper operations to comply with the regulation.

Columbia Analytical is currently analyzing for anthraquinone in samples for multiple organizations.

For more information on anthraquinone analysis, please contact Jeff Christian at 360-501-3316 or Ed Wallace at 360-577-7222.